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Effects of a structurally related substance on the crystallization of paracetamol

Ali SALEEMI, I.I. ONYEMELUKWE, Zoltan NAGY

《化学科学与工程前沿（英文）》 2013年第7卷第1期页码 79-87 doi: 10.1007/s11705-013-1308-7

摘要： Paracetamol (PCM) was crystallized from an isopropanol (IPA) solution containing various small amounts of metacetamol as an additive. The effect on the nucleation kinetics was studied by measuring the induction time to nucleation and the metastable zone width using focused beam reflectance measurements (FBRM) and attenuated total reflectance (ATR-UV/Vis) spectroscopy. Both the induction time and the metastable zone width were expressed as functions of the additive concentration. Small amounts of metacetamol (1–4 mol-%) were found to cause significant inhibition to the nucleation by extending both the induction time and the metastable zone width. A progressive change in the morphology of the paracetamol crystals from tabular to columnar habit was observed with increasing metacetamol concentration. The solvent also had a significant effect on the size of the paracetamol crystals as smaller crystals were obtained in IPA than in aqueous solution. The dissolution rate of paracetamol was improved by the incorporation of metacetamol with 4 mol-% having the most effect. A supersaturation control (SSC) approach was implemented for the PCM-IPA system with and without metacetamol in an attempt to control and obtain larger metacetamol-doped paracetamol crystals.

关键词： acetaminophen metacetamol crystallization metastable zone width induction time supersaturation control

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Simulation studies on metastable phase equilibria in the aqueous ternary systems (NaCl-MgCl

Tianlong DENG, Baojun ZHANG, Dongchan LI, Yafei GUO

《化学科学与工程前沿（英文）》 2009年第3卷第2期页码 172-175 doi: 10.1007/s11705-009-0048-1

摘要： The solubilities and densities of the aqueous metastable ternary systems (NaCl-MgCl -H O) and (KCl-MgCl -H O) at 308.15 K were determined by the isothermal evaporation method. On the basis of the experimental results, the phase diagrams for those systems were plotted. It was found that the former system belongs to the hydrate-I type with one invariant point of (NaCl+ MgCl ?6H O), two univariant curves, and two crystallization regions corresponding to halite (NaCl) and bischofite (MgCl ·6H O); and the latter system belongs to the type of incongruent-double salts with two invariant points of (KCl+ KCl·MgCl ·6H O) and (MgCl ·6H O+ KCl·MgCl ·6H O), three univariant curves, and three crystallization regions corresponding to potassium chloride (KCl), carnallite (KCl·MgCl ·6H O) and bischofite (MgCl ·6H O). No solid solutions were found in both systems.

关键词： green chemistry solar pond technique simulation metastable phase equilibrium solubility

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Calculation methods of the crack width and deformation for concrete beams with high-strength steel bars

Jianmin ZHOU, Shuo CHEN, Yang CHEN

《结构与土木工程前沿（英文）》 2013年第7卷第3期页码 316-324 doi: 10.1007/s11709-013-0211-0

摘要： Three groups of concrete beams reinforced with high-strength steel bars were tested, and the crack width and deformation of the specimens were observed and studied. To facilitate the predictions, two simplified formulations according to a theory developed by the first author were proposed. The advantages of the formulations were verified by the test data and compared with several formulas in different codes.

关键词： concrete beam high-strength steel bar crack width deformation

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Applying the multi-zone model in predicting the operating range of HCCI engines

Ming JIA, Maozhao XIE, Zhijun PENG,

《能源前沿（英文）》 2010年第4卷第3期页码 414-423 doi: 10.1007/s11708-010-0108-8

摘要： In this paper, a multi-zone model is developed to predict the operating range of homogeneous charge compression ignition (HCCI) engines. The boundaries of the operating range were determined by knock (presented by ringing intensity), partial burn (presented by combustion efficiency), and cycle-to-cycle variations (presented by the sensitivity of indicated mean effective pressure to initial temperature). By simulating an HCCI engine fueled with iso-octane, the knock and cycle-to-cycle variations predicted by the model showed satisfactory agreement with measurements made under different initial temperatures and equivalence ratios; the operating range was also well reproduced by the model. Furthermore, the model was applied to predict the operating range of the HCCI engine under different engine speeds by varying the intake temperatures and equivalence ratios. The potential to extend the operating range of the HCCI engine through two strategies, i.e., variable compression ratio and intake pressure boosting, was then investigated. Results indicate that the ignition point can be efficiently controlled by varying the compression ratio. A low load range can be extended by increasing the intake temperature while reducing the compression ratio. Higher intake temperatures and lower compression ratios can also extend the high load range. Boosting intake pressure is helpful in controlling the combustion of the HCCI engine, resulting in an extended high load range.

关键词： homogeneous charge compression ignition (HCCI) engine multi-zone operating range

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Influence of nozzle height to width ratio on ignition and NO

Liutao SUN, Yonghong YAN, Rui SUN, Zhengkang PENG, Chunli XING, Jiangquan WU

《能源前沿（英文）》 2021年第15卷第2期页码 431-448 doi: 10.1007/s11708-021-0726-3

摘要： To improve the ignition behavior and to reduce the high NO emissions of blended pulverized fuels (PF) of semicoke (SC), large-scale experiments were conducted in a 300 kW fired furnace at various nozzle settings, i.e., ratios (denoted by / ) of the height of the rectangular burner nozzle to its width of 1.65, 2.32, and 3.22. The combustion tests indicate that the flame stability, ignition performance, and fuel burnout ratio were significantly improved at a nozzle setting of / = 2.32. The smaller / delayed ignition and caused the flame to concentrate excessively on the axis of the furnace, while the larger / easily caused the deflection of the pulverized coal flame, and a high-temperature flame zone emerged close to the furnace wall. NO emissions at the outlet of the primary zone decreased from 447 to 354 mg/m (O = 6%), and the ignition distance decreased from 420 to 246 mm when the / varied from 1.65 to 3.22. Furthermore, the ratio (denoted by / ) of the strong reduction zone area to the combustion reaction zone area was defined experimentally by the CO concentration to evaluate the reduction zone. The / rose monotonously, but its restraining effects on NO formation decreased as / increased. The results suggested that in a test furnace, regulating the nozzle / conditions sharply reduces NO emissions and improves the combustion efficiency of SC blends possessing an appropriate jet rigidity.

关键词： rectangular jet burner nozzle height to width ratio ignition characteristics pyrolyzed semicoke (SC) and bituminous blend NO_x formation

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Numerical analysis of rotating stall characteristics in vaneless diffuser with large width-radius ratio

GAO Chuang, GU Chuangang, WANG Tong, DAI Zhengyuan

《能源前沿（英文）》 2008年第2卷第4期页码 457-460 doi: 10.1007/s11708-008-0071-9

摘要： A two-dimensional model, where the influence of wall boundary layers is neglected and inlet jet-wake velocity patterns are prescribed, was applied to simulate one vaneless diffuser with a large width-radius ratio. The impact of diffuser length, impeller blade number, etc. on the rotating stall was analyzed. Computational results show that a different mechanism does exist for diffusers with large width-radius ratios. Comparison with related conclusions and references is supportive of the model.

关键词： Comparison Computational two-dimensional influence different mechanism

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基于单位有效疏散宽度使用率的一种疏散设计评价方法

杨健鹏,张和平,潘峥,马宁,蒋为诚

《中国工程科学》 2006年第8卷第5期页码 94-97

摘要：

在建筑物的设计中，疏散通道的设计是非常重要的内容，设计是否合理关系到火灾时建筑物内的人员能否安全及时地疏散。但现行规范中并没有涉及到如何判断不同疏散方案的合理性。提出了一种评价方法，采用疏散通道出口单位有效疏散宽度使用率作为主要的评价指标，能较好地反映出不同设计方案之间的差异，并对如何调整疏散通道的位置使其更有利于人员的安全疏散有一定的指导作用。

关键词：火灾人员疏散单位有效疏散宽度使用率

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delamination on the stiffness of composite pipes under compressive transverse loading using cohesive zone

Sattar MALEKI, Roham RAFIEE, Abolfazl HASANNIA, Mohammad Reza HABIBAGAHI

《结构与土木工程前沿（英文）》 2019年第13卷第6期页码 1316-1323 doi: 10.1007/s11709-019-0555-1

摘要： The effect of delamination on the stiffness reduction of composite pipes is studied in this research. The stiffness test of filament wound composite pipes is simulated using cohesive zone method. The modeling is accomplished to study the effect of the geometrical parameters including delamination size and its position with respect to loading direction on stiffness of the composite pipes. At first, finite element results for stiffness test of a perfect pipe without delamination are validated with the experimental results according to ASTM D2412. It is seen that the finite element results agree well with experimental results. Then the finite element model is developed for composite pips with delaminated areas with different primary shapes. Thus, the effect of the size of delaminated region on longitudinal and tangential directions and also its orientation with respect to loading direction on delamination propagation and stiffness reduction of the pipes is assessed.

关键词： delamination composite pipes stiffness test cohesive zone method

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渤海辽东带地质认识的突破与金县1-1大油田的发现

邓运华

《中国工程科学》 2011年第13卷第10期页码 13-18

摘要：

辽东带系指渤海辽中凹陷的东部陡坡带及辽东凸起，被辽中及辽东凹陷所夹持。辽东带油源条件好，东营组储—盖条件优越，断鼻、断块圈闭发育。但在2002年之前的15年内，国内外公司在辽东带进行了长期研究和勘探，钻了12口探井，没有发现商业油气田。经过对辽东带油气地质条件3年的深入研究，对每口失利井原因进行了再次分析，认识到该带发育东营组及沙河街组两套主力成藏组合，控制东营组成藏的主要因素是油气运移，而沙河街组能否成藏关键是储层。在此认识指导下选择研究方向，评价有利目标，经钻探发现了金县1-1大油田，储量达1.5×10⁸ m³，充分显示了科研在油气勘探中的作用。

关键词：渤海辽东带金县1-1 地质认识大油田

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effects of mismatch fracture properties in encapsulation-based self-healing concrete using cohesive-zone

Luthfi Muhammad MAULUDIN, Chahmi OUCIF, Timon RABCZUK

《结构与土木工程前沿（英文）》 2020年第14卷第3期页码 792-801 doi: 10.1007/s11709-020-0629-0

摘要： Finite element analysis is developed to simulate the breakage of capsule in capsule-based self-healing concrete. A 2D circular capsule with different core-shell thickness ratios embedded in the mortar matrix is analyzed numerically along with their interfacial transition zone. Zero-thickness cohesive elements are pre-inserted into solid elements to represent potential cracks. This study focuses on the effects of mismatch fracture properties, namely fracture strength and energy, between capsule and mortar matrix into the breakage likelihood of the capsule. The extensive simulations of 2D specimens under uniaxial tension were carried out to investigate the key features on the fracture patterns of the capsule and produce the fracture maps as the results. The developed fracture maps of capsules present a simple but valuable tool to assist the experimentalists in designing appropriate capsule materials for self-healing concrete.

关键词： self-healing concrete interfacial zone capsule materials cohesive elements fracture maps

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Experimental investigation and design of aluminum columns with longitudinal welds

Yun WU, Qilin ZHANG

《结构与土木工程前沿（英文）》 2011年第5卷第3期页码 366-373 doi: 10.1007/s11709-011-0101-2

摘要： This paper presents an experimental investigation of longitudinally welded aluminum alloy I-section columns subjected to pure axial compression. The specimens were fabricated using 6061-T6 heat-treated aluminum alloy. The test program included 20 column tests which were separated into 2 test series of different types of welding sections. Each test series contained 10 columns. All the specimens were welded using the Tungsten Inert Gas welding method. The length of the specimens ranged from 442 to 2433 mm in order to obtain a column curve for each test series. The observed failure mode for the column tests includes mainly flexural buckling around the minor axis and the major axis by applying support except for one column (ZP1217-1) which buckled in the local zone and some columns which failed in the weld. The test strengths were compared with the design strengths predicted by the European Code and China Code for aluminum structures. The purpose of this paper is to present the tests results of two typically longitudinally welded I-section columns, and to check the accuracy of the design rules in the current specifications.

关键词： aluminum alloy longitudinal weld heat-affected zone (HAZ) reduced strength zone (RSZ) buckling column experimental study

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Cohesive zone model-based analyses of localized leakage of segmentally lined tunnels

《结构与土木工程前沿（英文）》 2023年第17卷第4期页码 503-521 doi: 10.1007/s11709-023-0927-4

摘要： This paper presents a novel approach for simulating the localized leakage behavior of segmentally lined tunnels based on a cohesive zone model. The proposed approach not only simulates localized leakage at the lining segment, but also captures the hydromechanically coupled seepage behavior at the segmental joints. It is first verified via a tunnel drainage experiment, which reveals its merits over the existing local hydraulic conductivity method. Subsequently, a parametric study is conducted to investigate the effects of the aperture size, stratum permeability, and spatial distribution of drainage holes on the leakage behavior, stratum seepage field, and leakage-induced mechanical response of the tunnel lining. The proposed approach yields more accurate results than the classical local hydraulic conductivity method. Moreover, it is both computationally efficient and stable. Localized leakage leads to reduced local ground pressure, which further induces outward deformation near the leakage point and slight inward deformation at its diametrically opposite side. A localized stress arch spanning across the leakage point is observed, which manifests as the rotation of the principal stresses in the adjacent area. The seepage field depends on both the number and location of the leakage zones. Pseudostatic seepage zones, in which the seepage rate is significantly lower than that of the adjacent area, appear when multiple seepage zones are considered. Finally, the importance of employing the hydromechanical coupled mechanism at the segment joints is highlighted by cases of shallowly buried tunnels subjected to surface loading and pressure tunnels while considering internal water pressure.

关键词： segmentally lined tunnel localized leakage cohesive element hydraulic behavior numerical modeling

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Simulation of cottonseed cake melt flow in metering zone of a single screw extruder

Hong HE, Jianguo ZHOU,

《化学科学与工程前沿（英文）》 2010年第4卷第3期页码 263-269 doi: 10.1007/s11705-009-0276-4

摘要： Research on the extrusion of natural polymers (food, feed, etc.) is relatively new due to the complex physicochemical transformations of raw materials, although plastics melt conveying and transport have been well studied. The structure and composition, rheological behavior as well as extrusion processing of natural polymer are much more complicated. In this study, a quasi-three-dimensional (3D) fluid flow model for non-Newtonian, non-isothermal and undeveloped temperature was developed, the model prediction being in reasonably good agreement with the experiment. Results show that the influence of moisture content, among other process variables, is the most significant, followed by screw speed. Some interaction exists between these two variables and the screw speed effect becomes marginal at high moisture contents. In addition, viscosity change in the channel was studied.

关键词： quasi-three-dimensional rheological viscosity processing influence

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基于粉碎区控制的钻孔爆破岩石-炸药匹配方法

冷振东,卢文波,严鹏,陈明,胡英国

《中国工程科学》 2014年第16卷第11期页码 28-35

摘要：

合理的炸药-岩石匹配关系对于提高炸药能量的有效利用率和改善破碎效果有着重要意义。传统上强调的波阻抗匹配理论并不合理，文章从爆破破碎机理出发，提出了一种岩石-炸药匹配的新方法，在保证相邻炮孔间岩石充分破碎的前提下，通过对粉碎区的合理控制来确定钻孔爆破最优的炸药性能参数。该方法可以直观地反映爆破破碎效果及能量有效利用率，可操作性强。考虑相邻炮孔爆炸荷载的联合作用，修正了钻孔爆破破坏分区计算模型。在此基础上，针对具体工程目标给出了混装炸药耦合装药条件下不同等级岩石的炸药性能匹配参数。

关键词：钻孔爆破粉碎区岩石-炸药匹配波阻抗匹配

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A modified zone model for estimating equivalent room thermal capacity

Hua CHEN, Xiaolin WANG

《能源前沿（英文）》 2013年第7卷第3期页码 351-357 doi: 10.1007/s11708-013-0254-x

摘要： The zone model has been widely applied in control analysis of heating, ventilation and air conditioning (HVAC) systems to achieve a high building efficiency. This paper proposed a modified zone model which is much simpler in the HVAC system simulation and has the similar accuracy to the complicated simulation model. The proposed model took into consideration the effect of envelop heat reservoir on the room indoor temperature by introducing the thermal admittance of the inner surfaces of the building enclosure. The thermal admittance for the building enclosure was developed based on the building thermal network analytical theory and transfer function method. The efficacy of the proposed model was demonstrated by comparing it with the complicated model — heat balance method (HTB2 program). The predicted results from the proposed model well agreed with those from the complicated simulation. The proposed model can then make the HVAC system dynamic simulation much faster and more acceptable for control design due to its simplicity and efficiency.

关键词： room model thermal network analysis transfer function heating ventilation and air conditioning (HVAC) system simulation